Synthesis of 4,7-substituted 1,10-phenanthrolines

A. R. Katritzky, Q. H. Long, N. Malhotra, T. A. Ramanarayanan, H. Vedage

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Abstract

4,7-Dialkylated-1,10-phenanthrolines 3a-f and 4c-d have been synthesized in high yields from 4,7-dimethyl-1,10-phenanthroline and 3,4,7,8-tetramethyl-1,10-phenanthroline, respectively, via lithiation followed by alkylation. These substituted phenanthrolines form complexes with lithium, and salts with proton acids, containing unusual ligand: cation ratios.

Original languageEnglish (US)
Pages (from-to)911-913
Number of pages3
JournalSynthesis
Issue number10
DOIs
StatePublished - Jan 1 1992
Externally publishedYes

All Science Journal Classification (ASJC) codes

  • Catalysis
  • Organic Chemistry

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    Katritzky, A. R., Long, Q. H., Malhotra, N., Ramanarayanan, T. A., & Vedage, H. (1992). Synthesis of 4,7-substituted 1,10-phenanthrolines. Synthesis, (10), 911-913. https://doi.org/10.1055/s-1992-26256