SYNTHESIS AND CHARACTERIZATION OF YBa2Cu3O7‐x SUPERCONDUCTORS

W. J. Weber; L. R. Pederson; J. M. Prince; K. C. Davis; G. J. Exarhos; G. D. Maupin; J. T. Prater; W. S. Frydrych; I. A. Aksay; B. L. Thiel; M. Sarikaya

doi:10.1111/j.1551-2916.1987.tb00111.x

SYNTHESIS AND CHARACTERIZATION OF YBa₂Cu₃O_7‐x SUPERCONDUCTORS

W. J. Weber, L. R. Pederson, J. M. Prince, K. C. Davis, G. J. Exarhos, G. D. Maupin, J. T. Prater, W. S. Frydrych, I. A. Aksay, B. L. Thiel, M. Sarikaya

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Abstract

Polycrystalline specimens of YBa₂Cu₃O_7‐x have been prepared by solid state reaction of the constituent metal oxides. The superconducting nature of the specimens has been characterized by magnetization, resistivity, and eddy current measurements. Onset temperatures for superconductivity exceed 88K. X‐ray and electron diffraction results confirm the orthorhombic crystal structure. Characteristic features have been observed by laser Raman spectroscopy. Copper valency has been determined by thermogravimetric analysis, iodometric titration, and x‐ray photoelectron spectroscopy. Additional evidence suggests that these materials are extremely sensitive to environmental conditions and handling. 1987 The American Ceramic Society

Original language	English (US)
Pages (from-to)	471-479
Number of pages	9
Journal	Advanced Ceramic Materials
Volume	2
Issue number	3 B
DOIs	https://doi.org/10.1111/j.1551-2916.1987.tb00111.x
State	Published - Jul 1987

All Science Journal Classification (ASJC) codes

Ceramics and Composites
Materials Chemistry

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10.1111/j.1551-2916.1987.tb00111.x

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title = "SYNTHESIS AND CHARACTERIZATION OF YBa2Cu3O7‐x SUPERCONDUCTORS",

abstract = "Polycrystalline specimens of YBa2Cu3O7‐x have been prepared by solid state reaction of the constituent metal oxides. The superconducting nature of the specimens has been characterized by magnetization, resistivity, and eddy current measurements. Onset temperatures for superconductivity exceed 88K. X‐ray and electron diffraction results confirm the orthorhombic crystal structure. Characteristic features have been observed by laser Raman spectroscopy. Copper valency has been determined by thermogravimetric analysis, iodometric titration, and x‐ray photoelectron spectroscopy. Additional evidence suggests that these materials are extremely sensitive to environmental conditions and handling. 1987 The American Ceramic Society",

author = "Weber, {W. J.} and Pederson, {L. R.} and Prince, {J. M.} and Davis, {K. C.} and Exarhos, {G. J.} and Maupin, {G. D.} and Prater, {J. T.} and Frydrych, {W. S.} and Aksay, {I. A.} and Thiel, {B. L.} and M. Sarikaya",

year = "1987",

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language = "English (US)",

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AU - Weber, W. J.

AU - Pederson, L. R.

AU - Prince, J. M.

AU - Davis, K. C.

AU - Exarhos, G. J.

AU - Maupin, G. D.

AU - Prater, J. T.

AU - Frydrych, W. S.

AU - Aksay, I. A.

AU - Thiel, B. L.

AU - Sarikaya, M.

PY - 1987/7

Y1 - 1987/7

N2 - Polycrystalline specimens of YBa2Cu3O7‐x have been prepared by solid state reaction of the constituent metal oxides. The superconducting nature of the specimens has been characterized by magnetization, resistivity, and eddy current measurements. Onset temperatures for superconductivity exceed 88K. X‐ray and electron diffraction results confirm the orthorhombic crystal structure. Characteristic features have been observed by laser Raman spectroscopy. Copper valency has been determined by thermogravimetric analysis, iodometric titration, and x‐ray photoelectron spectroscopy. Additional evidence suggests that these materials are extremely sensitive to environmental conditions and handling. 1987 The American Ceramic Society

AB - Polycrystalline specimens of YBa2Cu3O7‐x have been prepared by solid state reaction of the constituent metal oxides. The superconducting nature of the specimens has been characterized by magnetization, resistivity, and eddy current measurements. Onset temperatures for superconductivity exceed 88K. X‐ray and electron diffraction results confirm the orthorhombic crystal structure. Characteristic features have been observed by laser Raman spectroscopy. Copper valency has been determined by thermogravimetric analysis, iodometric titration, and x‐ray photoelectron spectroscopy. Additional evidence suggests that these materials are extremely sensitive to environmental conditions and handling. 1987 The American Ceramic Society

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SYNTHESIS AND CHARACTERIZATION OF YBa₂Cu₃O_7‐x SUPERCONDUCTORS

Abstract

All Science Journal Classification (ASJC) codes

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