Single-crystal CVD diamonds as small-angle X-ray scattering windows for high-pressure research

Suntao Wang, Yu Fei Meng, Nozomi Ando, Mark Tate, Szczesny Krasnicki, Chih Shiue Yan, Qi Liang, Joseph Lai, Ho Kwang Mao, Sol M. Gruner, Russell J. Hemley

Research output: Contribution to journalArticle

8 Scopus citations

Abstract

Small-angle X-ray scattering (SAXS) was performed on single-crystal chemical vapor deposition (CVD) diamonds with low nitrogen concentrations, which were fabricated by microwave plasma-assisted chemical vapor deposition at high growth rates. High optical quality undoped 500 m-thick single-crystal CVD diamonds grown without intentional nitrogen addition proved to be excellent as windows on SAXS cells, yielding parasitic scattering no more intense than a 7.5 m-thick Kapton film. A single-crystal CVD diamond window was successfully used in a high-pressure SAXS cell.

Original languageEnglish (US)
Pages (from-to)453-457
Number of pages5
JournalJournal of Applied Crystallography
Volume45
Issue number3
DOIs
StatePublished - Jun 2012

All Science Journal Classification (ASJC) codes

  • Biochemistry, Genetics and Molecular Biology(all)

Keywords

  • chemical vapor deposition
  • high pressure
  • microwave plasma
  • single-crystal diamonds
  • small-angle X-ray scattering

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    Wang, S., Meng, Y. F., Ando, N., Tate, M., Krasnicki, S., Yan, C. S., Liang, Q., Lai, J., Mao, H. K., Gruner, S. M., & Hemley, R. J. (2012). Single-crystal CVD diamonds as small-angle X-ray scattering windows for high-pressure research. Journal of Applied Crystallography, 45(3), 453-457. https://doi.org/10.1107/S0021889812010722