An improved protocol for the preparation of 3-pyridyl- and some arylboronic acids

Wenjie Li; Dorian P. Nelson; Mark S. Jensen; R. Scott Hoerrner; Dongwei Cai; Robert D. Larsen; Paul J. Reider

doi:10.1021/jo025792p

An improved protocol for the preparation of 3-pyridyl- and some arylboronic acids

Wenjie Li, Dorian P. Nelson, Mark S. Jensen, R. Scott Hoerrner, Dongwei Cai, Robert D. Larsen, Paul J. Reider

Research output: Contribution to journal › Article › peer-review

192 Scopus citations

Abstract

3-Pyridylboronic acid was prepared in high yield and bulk quantity from 3-bromopyridine via a protocol of lithium-halogen exchange and "in situ quench". This technique was further studied and evaluated on other aryl halides in the preparation of arylboronic acids.

Original language	English (US)
Pages (from-to)	5394-5397
Number of pages	4
Journal	Journal of Organic Chemistry
Volume	67
Issue number	15
DOIs	https://doi.org/10.1021/jo025792p
State	Published - Jul 26 2002
Externally published	Yes

All Science Journal Classification (ASJC) codes

Organic Chemistry

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10.1021/jo025792p

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title = "An improved protocol for the preparation of 3-pyridyl- and some arylboronic acids",

abstract = "3-Pyridylboronic acid was prepared in high yield and bulk quantity from 3-bromopyridine via a protocol of lithium-halogen exchange and {"}in situ quench{"}. This technique was further studied and evaluated on other aryl halides in the preparation of arylboronic acids.",

author = "Wenjie Li and Nelson, {Dorian P.} and Jensen, {Mark S.} and Hoerrner, {R. Scott} and Dongwei Cai and Larsen, {Robert D.} and Reider, {Paul J.}",

year = "2002",

month = jul,

day = "26",

doi = "10.1021/jo025792p",

language = "English (US)",

volume = "67",

pages = "5394--5397",

journal = "Journal of Organic Chemistry",

issn = "0022-3263",

publisher = "American Chemical Society",

number = "15",

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TY - JOUR

T1 - An improved protocol for the preparation of 3-pyridyl- and some arylboronic acids

AU - Li, Wenjie

AU - Nelson, Dorian P.

AU - Jensen, Mark S.

AU - Hoerrner, R. Scott

AU - Cai, Dongwei

AU - Larsen, Robert D.

AU - Reider, Paul J.

PY - 2002/7/26

Y1 - 2002/7/26

N2 - 3-Pyridylboronic acid was prepared in high yield and bulk quantity from 3-bromopyridine via a protocol of lithium-halogen exchange and "in situ quench". This technique was further studied and evaluated on other aryl halides in the preparation of arylboronic acids.

AB - 3-Pyridylboronic acid was prepared in high yield and bulk quantity from 3-bromopyridine via a protocol of lithium-halogen exchange and "in situ quench". This technique was further studied and evaluated on other aryl halides in the preparation of arylboronic acids.

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U2 - 10.1021/jo025792p

DO - 10.1021/jo025792p

M3 - Article

C2 - 12126436

AN - SCOPUS:0037178508

SN - 0022-3263

VL - 67

SP - 5394

EP - 5397

JO - Journal of Organic Chemistry

JF - Journal of Organic Chemistry

IS - 15

ER -

An improved protocol for the preparation of 3-pyridyl- and some arylboronic acids

Abstract

All Science Journal Classification (ASJC) codes

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